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KMID : 0370219740180020161
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Yakhak Hoeji
1974 Volume.18 No. 2 p.161 ~ p.164
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Synthesis of m-Hydroxy N-dimethylaniline Derivatives
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윤혜숙/Yun HS
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Abstract
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m-Hydroxyaniline was reported to be converted to m-methoxyaniline with dimethylsulfate. However while repeating the experiment with the same reaction condition, it was learned that the reaction product was not m-methoxyaniline but m-methoxy dimethylaniline. It was confirmed with nmr and ir spectrum and the comparison of bp and mp of the derivatives. Elemental analyses of the derivatives were also consistant with the fact that N-dimethylation along with O-methylation occurred.
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